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Insight into the Mechanism of the Conjugate Addition of the Sodium Carbanion to β-Chloroacrylic Ester.
The reaction of 1,3-dicarbonyl compounds with lithium di(isopropyl)amide to form lithium-stabilized carbanions is a useful method for building up β-dicarbonyls, which are structural motifs found in numerous biologically active compounds and natural products. Because of the importance of β-dicarbonyls in biology, medicinal chemistry, and the chemical industry, the development of general and efficient methods for their synthesis is highly desirable. Herein, we report a stoichiometric conjugate addition of the sodium carbanion to β-chloroacrylic ester. The reaction proceeds in a highly chemo- and regioselective manner to deliver a variety of enantioenriched β-dicarbonyl compounds in good to high yields with high levels of enantioselectivity.Could DMC Unite Superstars for an
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